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front-matter
2
Thermoset Composites: Preparation, Properties and Applications
2
Table of Contents
4
Preface
6
Energy Absorption of Natural Fibre Reinforced Thermoset Polymer Composites Materials for Automotive Crashworthiness: A Review
8
1.1 Introduction
9
1.2 Materials
11
1.3 Thermoset and thermoplastic composites
12
1.4 Matrix
13
1.5 Test methodologies
14
1.5.1 Quasi-static test
14
1.5.2 Dynamic test
14
1.6 Crashworthiness design
15
1.7 Crashworthiness prerequisites
17
1.8 Energy-absorbing thermoset composite structures
18
1.9 Assessing factors of energy absorption capability
19
1.9.1 Crush force efficiency (CFE)
19
1.9.2 Stroke efficiency (SE)
20
1.9.3 Initial failure indictor (IFI)
20
1.9.4 Specific energy absorption ES
20
1.10 Volumetric Energy absorption capability
21
1.11 Energy absorption
21
1.12 Literature survey
22
1.13 Conclusions
30
Acknowledgments
31
References
31
2
40
Wood Flour Filled Thermoset Composites
40
2.1 Introduction
41
2.2 Wood polymer composites
43
2.3 Wood flour composites (WFCs)
44
2.3.1 Processing of WFCs
45
2.3.2 Properties of WFCs
46
2.3.2.1 Mechanical properties
46
2.3.2.2 Surface roughness and wettability
48
2.3.2.3 Water absorption tests
49
2.3.2.4 Thermo-gravimetric analysis (TGA)
50
2.3.2.5 Differential scanning calorimetry (DSC)
51
2.3.2.6 Dynamic mechanical tests (DMA)
52
2.3.2.7 Creep test
52
2.3.2.8 Flammability characteristics
54
2.3.2.9 Tomography
55
2.3.3 Scanning electron microscopy (SEM) analysis
56
2.4 Practical applications
58
Conclusions
59
References
59
3
73
Experimental and Analysis of Jute Fabric with Silk Fabric Reinforced Polymer Composites
73
3.1 Introduction
74
3.2 Materials and methods
75
3.3 Preparation of composites
76
3.4 Experimentation
77
3.5 Results and discussions on experimentation
79
3.6 Analysis
82
Conclusion
85
References
86
4
88
Biosourced Thermosets for Lignocellulosic Composites
88
4.1 Introduction
89
4.2 Urea, also a natural material for wood adhesives
90
4.3 Tannin thermoset binders for wood adhesives
92
4.4 New technologies for industrial tannin adhesives
95
4.5 Tannin-Hexamethylenetetramine (Hexamine) adhesives and adhesives with alternative aldehydes
97
4.6 Hardening by tannins autocondensation
100
4.7 Lignin adhesives
102
4.8 Protein adhesives
105
4.9 Carbohydrate adhesives
105
4.10 Unsaturated oil adhesives
107
Conclusions
111
References
111
5
119
Hybrid Bast Fibre Strengthened Thermoset Composites
119
5.1 Introduction
120
5.2 Bast fibre
121
5.2.1 Surface morphology and elemental composition analysis
121
5.2.2 Structural composition and the physical properties of the bast fibre
123
5.2.3 Composition and the properties of the different bast fibre
124
5.3 Advantage and limitation of bast fibre as reinforcing material
125
5.4 Surface modification of bast fibres
126
5.5 Methods for surface modification of natural fibres
126
5.3.1 Physical methods
127
5.5.2 Chemical methods
127
5.5.2.1 Alkali treatment
127
5.5.2.2 Graft copolymerization
128
5.5.2.3 Acetylation
128
5.5.2.4 Treatment with isocyanate
128
5.5.2.5 Other chemical treatments
129
Conclusions
129
References
129
6
135
Nano-Carbon/Polymer Composites for Electromagnetic Shielding, Structural Mechanical and Field Emission Applications
135
6.1 Introduction
136
6.2 Shielding parameters of GNCs/Polyurethane nanocomposites
137
6.2.2 Characterizations and measurements
138
6.2.3 Analysis of microwave parameters
145
6.2.4 E?cient microwave absorbing properties:
148
6.3 Nanocomposite approach for structural engineering
153
6.3.1 GNCs as effective nanofiller
154
6.3.2 Dispersibility investigations: homogeneous distribution vs agglomeration and interfacial adhesion of GNCs
155
6.3.3 Raman mapping of GNCs nanocomposites
156
6.3.4 Optical imaging
157
6.3.5 Mechanical properties of GNCs/nanocomposites
158
6.3.3 Fracture mechanisms using fractography
162
6.3.4 Thermal and physical properties
164
6.4 MWNTs/nylon composite nanofibers by electrospinning
166
6.4.1 Synthesis of composite
167
6.4.2 Characterizations
168
6.4.3 I–V characteristic of the nanofiber composite
172
6.5 Carbon nanotube composite: Dispersion routes and field emission parameters
173
6.5.1 Synthesis of thin multiwall carbon nanotube composite
174
6.5.2 Characterization
176
6.3.3 Field emission parameters for the t–MWCNT–composite
180
Summary
183
References
185
7
196
Conductive Thermoset Composites
196
7.1 Introduction
197
7.2 Historical background of thermoset polymers
198
7.3 Method of Composite processing
201
7.4 Different types of CTC
204
7.4.1 Epoxy Based CTC
204
7.4.2 Polyurethane based CTC
204
7.4.3 Polyester based CTC
205
7.4.4 Polybenzoxanines based CTC
205
7.5 Properties of CTC
206
7.5.1 Thermal properties
206
7.5.2 Mechanical properties
206
7.5.3 Electrical properties
207
7.6 Applications of conductive thermoset composites
207
7.6.1 Electromagnetic interference (EMI) shielding
209
7.6.2 Anti-corrosive coatings
210
7.6.3 Shape memory application
211
7.6.4 Other applications
211
7.7 Problems and solution associated with CTC
212
Conclusion
214
Acknowledgment
214
References
215
8
224
Waterborne Thermosetting Polyurethane Composites
224
8.1 Introduction
225
8.2 PUD thermosetting composites
226
8.2.1 Inorganic oxide based PUD thermosetting composites
226
8.2.1.1 Silica-based PUD thermosetting composites
226
8.2.1.2 Titania (TiO2) based PUD thermosetting composites
231
8.2.1.3 Zinc oxide (ZnO) based PUD thermosetting composites
233
8.2.1.4 Other inorganic oxide-based PUD thermosetting composites
234
8.2.2 PUD thermosetting composites with metal (Ag and Au) nanoparticles
236
8.2.3 PUD/clay thermosetting composites
240
8.2.4 PUD/Carbohydrate thermosetting composites
242
8.2.4.1 Cellulose-based PUD thermosetting composites
242
8.2.4.2 Starch reinforced PUD thermosetting composites
245
8.2.5 PUD thermosetting composites reinforced with nanocarbon materials
247
8.2.5.1 Graphene oxide (GO), and reduced graphene oxide (rGO) based PUD thermosetting composites
248
8.2.5.2 Carbon nanotubes (CNTs) reinforced PUD thermosetting composites
249
Summary
250
Abbreviations
250
References
251
9
267
Classical Thermoset Epoxy Composites for Structural Purposes: Designing, Preparation, Properties and Applications
267
9.1 Introduction
269
9.2 Methods for modifying liquid epoxy compositions
271
9.2.1 Chemical modification of liquid epoxy compositions
272
9.2.2 Physico-chemical modification of liquid epoxy compositions
272
9.2.3 Methods of physical modification of liquid epoxy compositions
273
9.3 Physico-chemical aspects of the modification of epoxy polymers by dispersed and continuous fibrous fillers
275
9.3.1 Features of the formation of clusters in a polymer composite
275
9.3.2 Analysis of the surface interaction of fillers with epoxy oligomers
277
9.3.2.1 Surface interaction of inorganic fillers with epoxy oligomers
277
9.3.2.2 Surface interaction of organic fillers with epoxy oligomers
278
9.3.2.3 The mechanism of molecular interaction between epoxy polymer and filler
279
9.4 Effect of ultrasonic treatment regimes on the properties of epoxy polymers
280
9.4.1 Technological and operational properties of epoxy polymers
280
9.4.2 Physico-mechanical and technological properties of sonificated epoxy matrices
283
9.5 Ultrasonic intensification of prepregs formation
284
9.5.1 Process of capillary impregnation
284
9.5.2 Effect of ultrasonic modification regimes on the kinetics of impregnation of continuous fibrous fillers
285
9.6 Ultrasonic processing devices for liquid polymer systems
287
9.7 Modeling of the structure of oriented and woven fibrous materials
290
9.7.1 Physical models of a capillary-porous medium based on oriented fibrous fillers
291
9.8 Modeling of technical means for production of polymer composite materials
293
9.8.1 The technology of ultrasonic production of long-length epoxy composites
293
9.8.2 Modeling of technical means for thermoplastic production
295
9.9 Other applications of ultrasonic in the production of thermosets and thermoplastic
296
9.9.1 The effectiveness of ultrasonic treatment for the production of epoxy nanocomposites
296
9.9.2 Pepair technologies for the maintenance and restoration of polyethylene pipelines
297
Conclusions
299
References
300
10
307
A Review on Tribological Performance of Polymeric Composites Based on Natural Fibres
307
10.1 Introduction
308
10.2 Natural fibres
309
10.3 Polymer
310
10.4 Composite
313
10.5 Tribology
314
10.6 Friction and wear
317
Summary
332
Future Developments
336
References
337
back-matter
348
Keyword Index
348
About the Editors
349
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